HRID370655
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of succinic acid (0.22 g) in hot ethanol (10 ml) was added to a solution of 1-(1-naphthylmethyl)imidazole (0.4 g) in ethanol (5 ml). After boiling for 10 minutes, the solution was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-(1-naphthylmethyl)imidazole hydrogen succinate, m.p. 121°-123° C.
WORKUP
后处理
- customthe solution was evaporated under reduced pressure
- customto afford a white solid
- customRecrystallisation of the solid from ethyl acetate