HRID370655

反应详情

EQUATION

反应方程式

HRID 370655 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of succinic acid (0.22 g) in hot ethanol (10 ml) was added to a solution of 1-(1-naphthylmethyl)imidazole (0.4 g) in ethanol (5 ml). After boiling for 10 minutes, the solution was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-(1-naphthylmethyl)imidazole hydrogen succinate, m.p. 121°-123° C.

WORKUP

后处理

  1. customthe solution was evaporated under reduced pressure
  2. customto afford a white solid
  3. customRecrystallisation of the solid from ethyl acetate