HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → 1-(1-Naphthylmethyl)imidazole hydrogen succinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | 1H-Imidazole, 1-(1-naphthalenylmethyl)- | HCID 588244 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(1-Naphthylmethyl)imidazole hydrogen succinate | HCID 20275127 | — |
Reaction Steps
A solution of succinic acid (0.22 g) in hot ethanol (10 ml) was added to a solution of 1-(1-naphthylmethyl)imidazole (0.4 g) in ethanol (5 ml). After boiling for 10 minutes, the solution was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-(1-naphthylmethyl)imidazole hydrogen succinate, m.p. 121°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528195 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-d9d385d2aa66445b9c536c9bb5e62ab9 |
| Source note | uspto-grants-1985_07 |