HuagongsheHuagongshe Chemistry Print Report · For research reference only
91702-96-4 → HCID 3021853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 91702-96-4 | HCID 3021852 | — |
| Reactant | HCID 20275380 | HCID 20275380 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 3021853 | HCID 3021853 | — |
Reaction Steps
Following the procedure of Example 2, but substituting an equivalent amount of methyl 3-(2-acetylthiomethyl-propionamido)-picolinate, obtained as disclosed in Example 24, for methyl 2-(2-acetylthiomethyl-propionamido)-nicotinate and using ethyl acetate as eluent for the chromatography column, methyl 3-(2-mercaptomethyl-propionamido)-picolinate is obtained; m.p. 55°-56° C., from petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528296 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-e628734838394df48a45102e1cd69a3c |
| Source note | uspto-grants-1985_07 |