HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-Octyl 4-Chlorobenzimidoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-chloro-N-octylbenzamide | HCID 1721957 | — |
| Product | N-Octyl 4-Chlorobenzimidoyl Chloride | HCID 13477601 | 77% |
Reaction Steps
N-Octyl 4-chlorobenzamide (17.2 g, 64.2 mmole) and thionyl chloride (42.59 g, 358 mmole) were stirred and heated at reflux for one hour. The product was isolated by fractional distillation at reduced pressure (b.p. 70°-90° C. at 15 mm Hg) to yield 14.0 g (77%) of impure title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528382 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-d8717f55b0014481a130076770b05e2f |
| Source note | uspto-grants-1985_07 |