HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchloric Acid → Methyl 5-[(4-chlorophenyl)(octylimino)methyl]-1,4-dimethyl-1H-pyrrole-2-acetate Perchlorate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | Methyl 1,4-dimethyl-1H-pyrrole-2-acetate | HCID 13221886 | — |
| Reactant | N-Octyl 4-Chlorobenzimidoyl Chloride | HCID 13477601 | — |
| Product | Methyl 5-[(4-chlorophenyl)(octylimino)methyl]-1,4-dimethyl-1H-pyrrole-2-acetate Perchlorate | HCID 18598662 | — |
Reaction Steps
The title compound was prepared as in Example X from N-octyl 4-chlorobenzimidoyl chloride (1.44 g, 5 mmole), chlorosulfonic acid (0.58 g, 0.5 mmole), methyl 1,4-dimethyl-1H-pyrrole-2-acetate (0.84 g, 5 mmole), and 70% perchloric acid (0.79 g, 5.5 mmole) to yield 1.99 g (77%) of a red viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528382 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-b2134cae263f4ee09bbb0c1515447be2 |
| Source note | uspto-grants-1985_07 |