huagongshe.com
HRID370925

反应详情

EQUATION

反应方程式

HRID 370925 的结构方程式

REACTANTS

反应物

4
结构：[O-][Cl+3]([O-])([O-])O
HCID24247

Perchloric acid

HClO4

结构：O=S(=O)(O)Cl
HCID24638

Chlorosulfuric acid

HClO3S

结构：COC(=O)Cc1cc(C)cn1C
HCID13221886

Methyl 1,4-dimethyl-1H-pyrrole-2-acetate

C9H13NO2

结构：CCCCCCCCN=C(Cl)c1ccc(Cl)cc1
HCID13477601

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCN=C(c1ccc(Cl)cc1)c1c(C)cc(CC(=O)OC)n1C.[O-][Cl+3]([O-])([O-])O
HCID18598662

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as in Example X from N-octyl 4-chlorobenzimidoyl chloride (1.44 g, 5 mmole), chlorosulfonic acid (0.58 g, 0.5 mmole), methyl 1,4-dimethyl-1H-pyrrole-2-acetate (0.84 g, 5 mmole), and 70% perchloric acid (0.79 g, 5.5 mmole) to yield 1.99 g (77%) of a red viscous oil.