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HRID370926

反应详情

EQUATION

反应方程式

HRID 370926 的结构方程式

REACTANTS

反应物

4
结构：[O-][Cl+3]([O-])([O-])O
HCID24247

Perchloric acid

HClO4

结构：O=S(=O)(O)Cl
HCID24638

Chlorosulfuric acid

HClO3S

结构：CCOC(=O)Cc1cc(C)cn1C
HCID118467

Ethyl 1,4-dimethyl-1H-pyrrole-2-acetate

C10H15NO2

结构：CN=C(Cl)c1ccc(Cl)cc1
HCID12341506

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)Cc1cc(C)c(C(=NC)c2ccc(Cl)cc2)n1C.[O-][Cl+3]([O-])([O-])O
HCID20275542

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as in Example X from N-methyl 4-chlorobenzimidoyl chloride (7.52 g, 40 mmole), chlorosulfonic acid (0.47 g, 4 mmole), ethyl 1,4-dimethyl-1H-pyrrole-2-acetate (7.25 g, 40 mmole), and 70% perchloric acid (7.0 g, 48 mmole) to yield 6.6 g (38%) of a green solid, m.p. 126°-130° C. (dec).