HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 2817949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 2-bromopropionate | HCID 95576 | — |
| Reactant | 4-(3,5-Dichloro-pyridin-2-yloxy)-phenol | HCID 620880 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 2817949 | HCID 2817949 | — |
Reaction Steps
The above phenol (1.3 g, 5.08 mm), K2CO3 (1.05 g), methyl α-bromopropionate (0.85 ml, 1.5 eq) and acetone (20 ml) is refluxed for 8 hours. The mixture is then filtered and the filtrate concentrated to give oily methyl 2-[4-(3,5-dichloro-2-pyridyloxy)phenoxy]propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04529438 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-412c945b397b4104bc2ae1227d175687 |
| Source note | uspto-grants-1985_07 |