Silver → HCID 86740193, compound

Participants

Reaction Steps

Using the material from Example 2, 7 g of sodium dodecylsulfinate was dissolved in 300 ml H2O at 32° C. A silver solution was prepared by adding 7 ml of 3N AgNO3 to 200 ml H2O. With stirring between additions, the silver solution was added in four 50 ml portions to allow reaction to convert from the sodium salt to the silver salt. The reaction mixture at 32° C. gave a pH of 3.8 and a pAg of 6.3. The product was filtered, washed with four 100 ml portions of H2O, and dried.

Provenance & Evidence