Toluene → HCID 86739467, compound

Participants

Reaction Steps

To a solution containing 420 ml toluene, 195 ml methylene chloride, 75 ml ether and 5.15 g of succinimide is added 2.0 ml of water and 18.5 g of lithium perchlorate. The mixture is stirred for 18 hrs. The solids are removed by filtration, washed 2 times with 50 ml of cold 4:1, hexane:methylene chloride, and dried `in vacuo` to give 24.18 g of succinimide/lithium perchlorate complex.

Provenance & Evidence