Allyl chloride → HCID 22608987, compound
Reaction equation
[Na].[C:2]([NH:5][C:6]#[N:7])(=[O:4])[CH3:3].[CH2:8](Cl)[CH:9]=[CH2:10]>S1(CCCC1)(=O)=O>[C:6]([N:5]([CH2:10][CH:9]=[CH2:8])[C:2](=[O:4])[CH3:3])#[N:7]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
159.1 g (1.5 mols) of the sodium salt of acetylcyanamide and 137.8 g (1.5 mols+20% excess) of allyl chloride are reacted in 400 ml of sulfolane for 9 hours and 45 minutes at 70°-127° C. analogously to Example 1, and the mixture is worked up in accordance with Example 1. This gives 121.7 g (65.4% of theory) of a colourless distillate, boiling at 98° C./43 mbar.
Sources & evidence
- ORD record
- ord-99eb5e7c234f48768e87b7d4d5af6f0b
- Source dataset
- uspto-grants-1985_07
- Patent number
- US04529821
Reaction notes
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