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HRID371200

反应详情

EQUATION

反应方程式

HRID 371200 的结构方程式

REACTANTS

反应物

1
结构：CCCC[N+](CCCC)(CCCC)CCCC.O=C(N[C@H]1CN(S(=O)(=O)[O-])C1=O)OCc1ccccc1
HCID13575530

未命名化合物

PRODUCTS

生成物

1
结构：CCCC[N+](CCCC)(CCCC)CCCC.N[C@H]1CN(S(=O)(=O)[O-])C1=O
HCID13309502

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

(S)-2-Oxo-3-[[(phenylmethoxy)carbonyl]amino]-1-azetidinesulfonic acid, tetrabutylammonium salt (2 g; see Example 4) is dissolved in 100 ml of dimethylformamide and hydrogenated for about 30 minutes with 1 g of palladium on charcoal (10%) as catalyst. The catalyst is filtered off and the dimethylformamide is removed leaving the title compound as an oil.

WORKUP

后处理

  1. filtrationThe catalyst is filtered off
  2. customthe dimethylformamide is removed