HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,10-Dibromodecane → (((10-Bromodecyl)oxy)methyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,10-Dibromodecane | HCID 221483 | — |
| Reactant | CID 66729449 | HCID 66729449 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (((10-Bromodecyl)oxy)methyl)benzene | HCID 13478286 | — |
Reaction Steps
10-Benzyloxydecanyl bromide was prepared by reacting 100 g of 1,10-dibromodecane with an equimolar amount of sodium benzyloxide in tetrahydrofuran under reflux conditions, filtering the precipitated material, concentrating the filtrate and distilling the concentrated filtrate under reduced pressure. Yield 46 g. B.P. 185° to 189° C./3 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04530794 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-bb32426a91b04a2c9726f10be53ac35d |
| Source note | uspto-grants-1985_07 |