反应详情

10-Benzyloxydecanyl bromide was prepared by reacting 100 g of 1,10-dibromodecane with an equimolar amount of sodium benzyloxide in tetrahydrofuran under reflux conditions, filtering the precipitated material, concentrating the filtrate and distilling the concentrated filtrate under reduced pressure. Yield 46 g. B.P. 185° to 189° C./3 mmHg.

1. filtrationfiltering the precipitated material
2. concentrationconcentrating the filtrate
3. distillationdistilling the concentrated filtrate under reduced pressure