Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Silver Nitrate | HCID 24470 | — |
| Reactant | HCID 13303848 | HCID 13303848 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 131714282 | HCID 131714282 | — |
Reaction Steps
To a 50 ml flask equipped with a nitrogen atmosphere add 10 ml of methanol and 460 mg of (3S,4R)-1-(allyloxycarbonylmethyl)-3-(1-hydroxyethyl)-4-(triphenylmethylthio)azetidin-2-one. To this system add 160 mg silver nitrate and 0.15 ml of pyridine. Stir the system at 20° C. for 1 hour. Stop the reaction and remove the methanol by stripping to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04530793 |
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| Source dataset | uspto-grants-1985_07 |
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| ORD ID | ord-642b7ea79c7542e5acad79d1b53e00b8 |
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| Source note | uspto-grants-1985_07 |
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