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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 371269Generated: October 31, 2026

Methanol → HCID 131714282, compound

https://huagongshe.com/reaction/371269

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSilver NitrateHCID 24470—
ReactantHCID 13303848HCID 13303848—
SolventPyridineHCID 1049—
ProductHCID 131714282HCID 131714282—

Reaction Conditions

Temperature20 °C

Reaction Steps

To a 50 ml flask equipped with a nitrogen atmosphere add 10 ml of methanol and 460 mg of (3S,4R)-1-(allyloxycarbonylmethyl)-3-(1-hydroxyethyl)-4-(triphenylmethylthio)azetidin-2-one. To this system add 160 mg silver nitrate and 0.15 ml of pyridine. Stir the system at 20° C. for 1 hour. Stop the reaction and remove the methanol by stripping to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04530793
Source datasetuspto-grants-1985_07
ORD IDord-642b7ea79c7542e5acad79d1b53e00b8
Source noteuspto-grants-1985_07