HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 13720696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 8-Aminoquinoline | HCID 11359 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13720696 | HCID 13720696 | — |
Reaction Steps
8-Aminoquinoline (2.0 g., Pfaltz & Bauer, A28560) in methylene chloride (10 ml) was added dropwise to a 0° C. solution of 2.2M phosgene in methylene chloride (12 ml). The resulting precipitate was filtered and dried. The dark solid thus obtained is unstable and in practice it was immediately used in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04530931 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-dc6bfa4b738245a2b3ec7f3564126b2c |
| Source note | uspto-grants-1985_07 |