Hydrochloric Acid → HCID 53911695, compound

Participants

Reaction Steps

A solution of 0.10 g of potassium t-butoxide in 3 ml of t-butanol was added drop-by-drop over 5 minutes to a solution of 0.23 g of 15 in 10 ml of t-butanol under nitrogen, at room temperature. After 40 minutes, the mixture was poured into 2% hydrochloric acid saturated with sodium chloride and the resulting mixture was extracted with methylene chloride. The solvent was purified over silica gel to give 24, as a solid, m.p.: 90°-92° C.

Provenance & Evidence