HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53882321, compound → 3-Chloro-1,4-dihydro-2,6-dimethyl-5-nitro-4-(3-nitrophenyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53882321 | HCID 53882321 | — |
| Reactant | 1-Nitroprop-1-en-2-amine | HCID 71404712 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Chloro-1,4-dihydro-2,6-dimethyl-5-nitro-4-(3-nitrophenyl)pyridine | HCID 13242099 | — |
Reaction Steps
0.1 mol of 2-amino-1-nitro-prop-1-ene and 0.1 mol of 2-chloro-1-(3-nitrophenyl)-but-1-ene-3-one were heated in boiling ethanol, analogously to Example 18. 3-Chloro-1,4-dihydro-2,6-dimethyl-5-nitro-4-(3-nitrophenyl)pyridine of melting point 198° C. (decomposition) was obtained. Yield:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04532248 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-1be33fe1ce1c4f71929282c25223a0bb |
| Source note | uspto-grants-1985_07 |