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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 371443Generated: October 31, 2026

Formaldehyde → Dibenzyl ether

https://huagongshe.com/reaction/371443

Reaction equation

Participants

RoleNameHCIDCharge
ReactantFormaldehydeHCID 712—
ReactantPhenolHCID 996—
ReactantLead naphthenatesHCID 25021832—
ProductDibenzyl etherHCID 7657—

Reaction Conditions

Temperature130 °C

Reaction Steps

A benzyl ether-type phenolic resin was prepared in a known method by the condensation reaction of 470 kg of phenol and 479 kg of 47% formalin in the presence of lead naphthenate as the catalyst followed by the removal of the unreacted phenol and formaldehyde as well as water and the like volatile matter under reduced pressure with heating up to a maximum temperature of 130° C. The thus obtained phenolic resin was solid at room temperature and had a softening point of 60° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04532271
Source datasetuspto-grants-1985_07
ORD IDord-c3319b7dc6e4473790f0d217eb8d7bc0
Source noteuspto-grants-1985_07