HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 20273406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2-Chloro-N-{4-[(4-nitrophenyl)sulfanyl]phenyl}acetamide | HCID 226891 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20273406 | HCID 20273406 | — |
Reaction Steps
A mixture of 3.0 g of 2-chloro-4'-(p-nitrophenylthio)acetanilide and a 4.0% aqueous solution of methylamine in ethanol was refluxed for 4 hours. The solvent was evaporated, the residue dissolved on dichloromethane and crystallized by the addition of hexane, giving 2.25 g of the desired product, mp 86°-89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04532349 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-36d51003b7674819b4c594c22681e699 |
| Source note | uspto-grants-1985_07 |