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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 371508Generated: October 30, 2026

Water → HCID 13478030, compound

https://huagongshe.com/reaction/371508

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium AzideHCID 33557—
ReactantHCID 13478029HCID 13478029—
SolventEthanolHCID 702—
ProductHCID 13478030HCID 1347803058.9%

Reaction Steps

A mixture of 2.0 g of 2-chloro-4'-(m-chlorophenylsulfonyl)acetanilide, 0.41 g of sodium azide, 20 ml of water and 40 ml of ethanol was refluxed for 3.5 hours and then evaporated to dryness. The residue was crystallized from ethanol, giving 1.2 g of 2-azido-4'-(m-chlorophenylsulfonyl)acetanilide, mp 125°-126° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04532349
Source datasetuspto-grants-1985_07
ORD IDord-befec4322a844fe492fbc07516dc2189
Source noteuspto-grants-1985_07