HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Pyridinecarbonitrile, 3,5,6-trichloro-4-hydrazino-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Tetrachloropicolinonitrile | HCID 87323 | — |
| Reactant | 3,5,6-Trichloro-4-hydrazinylpyridine-2-carboxylic acid | HCID 1383439 | — |
| Product | 2-Pyridinecarbonitrile, 3,5,6-trichloro-4-hydrazino- | HCID 1898616 | — |
Reaction Steps
The 3,5,6-trichloro-4-hydrazinopicolinic acid can be prepared in a variety of ways. In one such method, tetrachloropicolinonitrile is reacted with hydrazine in the presence of a reaction medium and hydrogen chloride acceptor. The 3,5,6-trichloro-4-hydrazinopicolinonitrile product thus formed is reacted with an acid hydrolysis agent to prepare 3,5,6-trichloro-4-hydrazinopicolinic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087431 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-97649d3c115f482aa74d07833af85f6b |
| Source note | uspto-grants-1978_05 |