HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20355358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-(2-Hydroxyethyl)piperazine | HCID 7677 | — |
| Reactant | HCID 20355346 | HCID 20355346 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20355358 | HCID 20355358 | — |
Reaction Steps
A solution of 7,10-bis(methylthio)-4H-thieno[3,4-b][1,5]benzodiazepine in excess N-(2-hydroxyethyl)-piperazine and glacial acetic acid is heated at 140°-160° C. for 2 days. The solution is poured into water and the product is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087421 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-698537d82f57408eae944493af5d5929 |
| Source note | uspto-grants-1978_05 |