HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20355353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | HCID 20355322 | HCID 20355322 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20355353 | HCID 20355353 | — |
Reaction Steps
A solution of 6-nitro-10-(methylthio)-4H-thieno[3,4-b][1,5]benzodiazepine in excess N-benzylpiperazine and glacial acetic acid is heated at 140°-160° C. for 2 days. The solution is poured into water and the product is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087421 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-d6895fde147a40409350b6a812bd52ee |
| Source note | uspto-grants-1978_05 |