HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20355331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | HCID 20355345 | HCID 20355345 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20355331 | HCID 20355331 | — |
Reaction Steps
A solution of 6-methylsulfonyl-10-(methylthio)-4H-thieno[3,4-b][1,5]benzodiazepine in excess piperazine and glacial acetic acid is heated in a bomb at 150° C. for 2 days. The solution is poured into water and the product is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087421 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-d76a83fadcf14ba08d19296bcb25fff7 |
| Source note | uspto-grants-1978_05 |