HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 4-Ethyl-N-methoxy-2,6-dinitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chloro-3,5-dinitrotoluene | HCID 78918 | — |
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Product | 4-Ethyl-N-methoxy-2,6-dinitroaniline | HCID 21329888 | — |
Reaction Steps
Following the same general procedure of Example 2 and using 21.6 g. (0.1 mole) of 2,6-dinitro-4-methylchlorobenzene, 12.5 g. (0.15 mole) of methoxyamine hydrochloride, and 25.25 g. (0.25 mole) of triethylamine, the following additional compound was prepared:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087460 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-e0058999847d4b7e9fc115ed115fe4bb |
| Source note | uspto-grants-1978_05 |