HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 19906125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 86735669 | HCID 86735669 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19906125 | HCID 19906125 | — |
Reaction Steps
1 g. of Monomethyl propylcarbamoylmethylphosphonate was suspended in 10 ml. of hydrogen bromide in glacial acetic acid. The solution was allowed to stand overnight at room temperature. The solution was then concentrated to a viscous oil under reduced pressure. Upon the addition of methanol, the compound crystallized; m.p. 155°-160° C.; yield, 47%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087522 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-ef0ec5d26e04419b88d7a744fa20f896 |
| Source note | uspto-grants-1978_05 |