Thionyl Chloride → HCID 20355935, compound

HRID 371718Notes

Reaction equation

HRID 371718 reaction equation
S(Cl)([Cl:3])=O.O[CH:6]([NH:12][CH:13]=[O:14])[C:7]([Cl:11])([Cl:10])[CH2:8][Cl:9]>>[Cl:3][CH:6]([NH:12][CH:13]=[O:14])[C:7]([Cl:11])([Cl:10])[CH2:8][Cl:9]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20355973HCID 20355973, compound

Product 1

HCID 20355935HCID 20355935, compound

Procedure

Thionyl chloride was poured over 20.6 gm of N-(1-hydroxy-2,2,3-trichloro-n-propyl)-formamide, and the mixture was refluxed for 15 minutes. Subsequently, the excess thionyl chloride was distilled off, and the residue was recrystallized from benzene/petroleum ether, m.p. 55°-57° C.

Workup

  1. temperaturethe mixture was refluxed for 15 minutes
  2. distillationSubsequently, the excess thionyl chloride was distilled off
  3. customthe residue was recrystallized from benzene/petroleum ether, m.p. 55°-57° C.

Sources & evidence

ORD record
ord-b94f4ff194134f0aa6795dd54cee79d9
Source dataset
uspto-grants-1978_05
Patent number
US04087533

Reaction notes

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