HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20355935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20355973 | HCID 20355973 | — |
| Product | HCID 20355935 | HCID 20355935 | — |
Reaction Steps
Thionyl chloride was poured over 20.6 gm of N-(1-hydroxy-2,2,3-trichloro-n-propyl)-formamide, and the mixture was refluxed for 15 minutes. Subsequently, the excess thionyl chloride was distilled off, and the residue was recrystallized from benzene/petroleum ether, m.p. 55°-57° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087533 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-b94f4ff194134f0aa6795dd54cee79d9 |
| Source note | uspto-grants-1978_05 |