HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 60142-97-4 | HCID 21321132 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22065262 | HCID 22065262 | — |
Reaction Steps
In an anologous manner as described in Example 2 1-aminomethyl-1-cycloheptane acetic acid hydrochloride is esterified with methanol in the presence of hydrogen chloride. After working up and crystallisation from isopropanol/ether/hexane, methyl 1-aminomethyl-1-cycloheptane-acetate is obtained as hydrochloride in the form of colourless crystals having a melting point of 115° - 116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087544 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-8ec7721793964462b92a3bf03a970a0e |
| Source note | uspto-grants-1978_05 |