HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20356147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 20356074 | HCID 20356074 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 20356147 | HCID 20356147 | — |
Reaction Steps
A solution of 300 mg. of 5-(2-thenoyl)-1,2-dihydro-3H-pyrrolo[1,2-a]pyrrole-1-carboxylic acid in 5 ml. of isoamyl alcohol is saturated with hydrogen chloride. After 24 hours, the excess alcohol is distilled off in vacuum and the residue purified by chromatography on alumina to yield isoamyl 5-(2-thenoyl)-1,2-dihydro-3H-pyrrolo[1,2-a]pyrrole-1-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087539 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-8e6658a6bafb4b1d9bfe6603f36821ce |
| Source note | uspto-grants-1978_05 |