HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 2-Amino-N,N-dimethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Amino-5-methoxyphenyl)methanol | HCID 13756678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-N,N-dimethyl-5-methoxy-benzylamine | HCID 20319028 | — |
Reaction Steps
2-Amino-N,N-dimethyl-5-methoxy-benzylamine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chloride and dimethylamine analogous to Example 1. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3280 cm-1NH2 ; 3420 cm-1NH2 ; 2780 cm-1N(CH3)2 ; 2830 cm-1OCH3 ; 1600 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-368b7ede9f9147e09b447a441c60cf3a |
| Source note | uspto-grants-1978_05 |