HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → 2-Amino-N,N-diethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Amino-5-methoxyphenyl)methanol | HCID 13756678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-N,N-diethyl-5-methoxy-benzylamine | HCID 422009 | — |
Reaction Steps
2-Amino-N,N-diethyl-5-methoxy-benzylamine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chloride and diethylamine analogous to Example 1. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3260 cm-1NH2 ; 3410 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-ethyl; 1510 cm-1C=C; 1600 cm-1C=C. EXAMPLE 123
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-4e450f9dd0c142fc9dfdf355e53e373e |
| Source note | uspto-grants-1978_05 |