HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → N-(2-Amino-3-bromo-5-methoxy-benzyl)-morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | N-(2-Amino-5-methoxy-benzyl)-morpholine | HCID 20318983 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(2-Amino-3-bromo-5-methoxy-benzyl)-morpholine | HCID 20319084 | — |
Reaction Steps
N-(2-Amino-3-bromo-5-methoxy-benzyl)-morpholine was prepared from N-(2-amino-5-methoxy-benzyl)-morpholine and bromine analogous to Exanple 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3280 cm-1NH2 ; 3420 cm-1NH2 ; 2830 cm-1OCH3 ; 2810 cm-1N-alkyl; 1480 cm-1C= C; 1590 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-2fd6073daeaa47f38fa5fa906d8a8a63 |
| Source note | uspto-grants-1978_05 |