Bromine → HCID 20319136, compound

HRID 371876Notes

Reaction equation

HRID 371876 reaction equation
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][C:3]=1[CH2:4][N:5]([CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)[CH3:6].[Br:19]Br>C(Cl)Cl>[NH2:1][C:2]1[C:16]([Br:19])=[CH:15][C:14]([O:17][CH3:18])=[CH:13][C:3]=1[CH2:4][N:5]([CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)[CH3:6]

Participants

4

Reactant 2

HCID 24408BromineHCID 54118647HCID 54118647, compound

Product 1

HCID 20319136HCID 20319136, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

2-Amino-3-bromo-N-cyclohexyl-5-methoxy-N-methyl-benzylamine was prepared from 2-amino-N-cyclohexyl-5-methoxy-N-methyl-benzylamine and bromine analogous to Example 9. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride): 3240 cm-1NH2 ; 3410 cm-1NH2 ; 2860 cm-1 aliphatic hydrocarbon; 2940 cm-1 aliphatic hydrocarbon; 2830 cm-1OCH3 ; 2800 cm-1N-alkyl; 1480 cm-1C=C; 1590 cm-1C=C.

Sources & evidence

ORD record
ord-46377ff53e8244ad92889625c28afcb7
Source dataset
uspto-grants-1978_05
Patent number
USRE029628

Reaction notes

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