HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 20319136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 54118647 | HCID 54118647 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20319136 | HCID 20319136 | — |
Reaction Steps
2-Amino-3-bromo-N-cyclohexyl-5-methoxy-N-methyl-benzylamine was prepared from 2-amino-N-cyclohexyl-5-methoxy-N-methyl-benzylamine and bromine analogous to Example 9. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride): 3240 cm-1NH2 ; 3410 cm-1NH2 ; 2860 cm-1 aliphatic hydrocarbon; 2940 cm-1 aliphatic hydrocarbon; 2830 cm-1OCH3 ; 2800 cm-1N-alkyl; 1480 cm-1C=C; 1590 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-46377ff53e8244ad92889625c28afcb7 |
| Source note | uspto-grants-1978_05 |