HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319198 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319233 | — |
Reaction Steps
2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine was prepared from 2-amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine and bromine analogous to Example 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3240 cm-1NH2 ; 3410 cm-1NH2 ; 2860 cm-1 aliphatic hydrocarbon; 2940 cm-1 aliphatic hydrocarbon; 2830 cm-1OCH3 ; 2800 cm-1N-ethyl (shoulder); 1480 cm-1C=C; 1590 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-2428526235f242e6b557e7e2c0e87d7b |
| Source note | uspto-grants-1978_05 |