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HRID371878

反应详情

EQUATION

反应方程式

HRID 371878 的结构方程式

REACTANTS

反应物

3
结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：COc1ccc(N)c(CO)c1
HCID13756678

(2-Amino-5-methoxyphenyl)methanol

C8H11NO2

PRODUCTS

生成物

1
结构：COc1ccc(N)c(CN2CCOCC2)c1
HCID20318983

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

N-(2-Amino-5-methoxy-benzyl)-morpholine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chloride and morpholine analogous to Example 1. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride) 3280 cm-1NH2 ; 3410 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-alkyl; 1500 cm-1C=C; 1600 cm -1 C=C.