HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → N-(2-Amino-5-methoxy-benzyl)-morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Amino-5-methoxyphenyl)methanol | HCID 13756678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(2-Amino-5-methoxy-benzyl)-morpholine | HCID 20318983 | — |
Reaction Steps
N-(2-Amino-5-methoxy-benzyl)-morpholine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chloride and morpholine analogous to Example 1. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride) 3280 cm-1NH2 ; 3410 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-alkyl; 1500 cm-1C=C; 1600 cm -1 C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-9a7a426fd34c4806a4364818591e41c4 |
| Source note | uspto-grants-1978_05 |