HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-BOC-ethylenediamine → HCID 19934801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Reactant | HCID 19934797 | HCID 19934797 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 19934801 | HCID 19934801 | — |
Reaction Steps
4 g (0.0095 mol) of methyl 2-[[3-[4-(5-chloro-2-methoxyphenyl)piperain-1-yl]propyl]amino]-pyrazine-5-carboxylate and 3.05 g (0.02 mol) of 1,1-dimethylethyl 2-aminoethylcarbamate are introduced into 10 ml of 2-propanol in a 0.5 l round-bottomed flask and the mixture is heated at reflux for 2 days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420130 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-2aed04866ac14fcbad5c553531ab1af8 |
| Source note | uspto-grants-1995_05 |