HRID371947
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a suspension of 3-acetyl-1-phenyl-3-azabicyclo[3.1.0]hexane in concentrated sulfuric acid is added concentrated nitric acid during 15 minutes at 0°-10° C. The resulting mixture is stirred at room temperature for 15 minutes and then poured onto ice. The product, 3-acetyl-1-(p-nitrophenyl)-3-azabicyclo[3.1.0]hexane, is collected by filtration.
WORKUP
后处理
- additionpoured onto ice
- filtrationThe product, 3-acetyl-1-(p-nitrophenyl)-3-azabicyclo[3.1.0]hexane, is collected by filtration