HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 20352244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 1-(4-Methoxyphenyl)-3-azabicyclo[3.1.0]hexane | HCID 12719855 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Product | HCID 20352244 | HCID 20352244 | — |
Reaction Steps
To a stirred mixture of 1-(p-methoxyphenyl)-3-azabicyclo[3.1.0]hexane in benzene and aqueous sodium carbonate is added acetyl chloride and the mixture is stirred at ambient temperature for 18 hours. Benzene is removed by evaporation under reduced pressure, and filtration of the residual mixture gives 3-acetyl-1-(p-methoxyphenyl)-3-azabicyclo[3.1.0]hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04088652 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-ed16a27b620341238b26e7bb977b0c6d |
| Source note | uspto-grants-1978_05 |