HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178449602, compound → HCID 178479356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178449602 | HCID 178449602 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178479356 | HCID 178479356 | — |
Reaction Steps
A mixture of 32.1 g. (0.106 moles) of 1-(2,6-dichlorophenylamidino)-3-(t-butyl)urea and 200 ml of conc. hydrochloric acid is refluxed for 1/2 hour. The reaction mixture is cooled, filtered and washed with 10 ml of 1:1 HCl/H2O and dried. The product is then recrystallized from ethanol-ether to obtain (2,6-dichlorophenylamidino)urea hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04088785 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-38999293618c4c159ce124ffe5460606 |
| Source note | uspto-grants-1978_05 |