Azobisisobutyronitrile → HCID 86735707, compound

Participants

Reaction Steps

3.56 g of acrylamide and 7.15 g of N-vinyl-t-butylcarbamate were dissolved in 90 mls of benzene. 0.01 g of 2,2'-azobis-[2-methylpropionitrile] was added and the solution was polymerized under N2 in a sealed tube for 24 hours. The resultant viscous liquid was precipitated in acetone and the precipitate was separated and dried under vacuum at 50° C.

Provenance & Evidence