Azobisisobutyronitrile → HCID 86735707, compound

HRID 372144Notes

Reaction equation

HRID 372144 reaction equation
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH:6]([N:8]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:9](=[O:11])[O-:10])=[CH2:7].N(C(C)(C)C#N)=NC(C)(C)C#N>C1C=CC=CC=1>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH:6]([N:8]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:9](=[O:10])[O-:11])=[CH2:7]

Participants

5

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 6579AcrylamideHCID 86735708HCID 86735708, compound

Product 1

HCID 86735707HCID 86735707, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

3.56 g of acrylamide and 7.15 g of N-vinyl-t-butylcarbamate were dissolved in 90 mls of benzene. 0.01 g of 2,2'-azobis-[2-methylpropionitrile] was added and the solution was polymerized under N2 in a sealed tube for 24 hours. The resultant viscous liquid was precipitated in acetone and the precipitate was separated and dried under vacuum at 50° C.

Workup

  1. customthe solution was polymerized under N2 in a sealed tube for 24 hours
  2. customThe resultant viscous liquid was precipitated in acetone
  3. customthe precipitate was separated
  4. customdried under vacuum at 50° C.

Sources & evidence

ORD record
ord-b0871b66050f4e6bb19a913ea530fffb
Source dataset
uspto-grants-1978_05
Patent number
US04089688

Reaction notes

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