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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 37215Generated: October 25, 2026

Potassium Carbonate → HCID 21472340, compound

https://huagongshe.com/reaction/37215

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 12022872HCID 12022872—
Reactant1-(4-Bromophenyl) 2-heptyn-1-oneHCID 54449136—
SolventDimethylformamideHCID 6228—
ProductHCID 21472340HCID 21472340—

Reaction Steps

A mixture of 11.4 g of the product of Stage A of Example 1, 250 ml of dimethylformamide and 9.81 g of 1-amino 2-methylpyridinium 2,4,6-trimethyl-benzene sulfonate (Synthesis, 1977, page 1, TAMURA, et al.) and 5.11 g of potassium carbonate were stirred for 5 hours at ambient temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05420138
Source datasetuspto-grants-1995_05
ORD IDord-0bc925d40dea443fb918fe585560b973
Source noteuspto-grants-1995_05