Methyldichlorosilane → HCID 18951489, compound

HRID 372173Notes

Reaction equation

HRID 372173 reaction equation
[CH3:1][SiH:2]([Cl:4])[Cl:3].[F:5][C:6]([F:13])([C:9]([F:12])([F:11])[F:10])[CH:7]=[CH2:8]>>[F:5][C:6]([F:13])([C:9]([F:12])([F:11])[F:10])[CH2:7][CH2:8][Si:2]([CH3:1])([Cl:4])[Cl:3]

Participants

3

Reactant 2

HCID 6376MethyldichlorosilaneHCID 789903,3,4,4,4-Pentafluorobut-1-ene

Product 1

HCID 18951489HCID 18951489, compoundYield 91%

Procedure

Into a reaction vessel were put 200 g of methyldichlorosilane and the same amount of the same binary catalyst as in Example 1, followed by the addition of 242 g of 3,3,4,4,4-pentafluorobutene. After the completion of the reaction at 70° C under 6 atmospheres, the reaction product was subjected to distillation to produce 3,3,4,4,4-pentafluorobutylmethyldichlorosilane (Boiling point: 130° C) at the yield 91% of the theoretical.

Workup

  1. customInto a reaction vessel were put
  2. customAfter the completion of the reaction at 70° C under 6 atmospheres
  3. distillationthe reaction product was subjected to distillation

Sources & evidence

ORD record
ord-ee0968b9fad94e75b97ba22b7da746a2
Source dataset
uspto-grants-1978_05
Patent number
US04089882

Reaction notes

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