HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20528114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 13487034 | HCID 13487034 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 20528114 | HCID 20528114 | — |
Reaction Steps
A solution of 300 mg. of 5-p-toluoyl-1,2-dihydro-3H-pyrrolo[1,2-a]pyrrole-1-carboxylic acid in 5 ml. of isoamyl alcohol is saturated with hydrogen chloride. After 24 hours, the excess alcohol is distilled off in vacuo and the residue purified by chromatography on alumina, to yield isoamyl 5-p-toluoyl-1,2-dihydro-3H-pyrrolo[1,2-a]pyrrole-1-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04089969 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-ca7bf19ba4534436b31d6e634d083289 |
| Source note | uspto-grants-1978_05 |