HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylcarbamyl fluoride → N-Methyl-N-(n-Octylthiosulfenyl)Carbamoyl Fluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylcarbamyl fluoride | HCID 12545956 | — |
| Reactant | n-Octylthiosulfenylchloride | HCID 20325288 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-Methyl-N-(n-Octylthiosulfenyl)Carbamoyl Fluoride | HCID 23333005 | — |
Reaction Steps
Prepared as above by adding 25.2 g triethylamine to a solution of 48.0 g. n-octylthiosulfenylchloride and 19.26 g N-methylcarbamoyl fluoride. b.p. 110°-118° C/0.2 Torr. ND21 1.4900.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091016 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-44a631b71869410598a19aae6c2cc912 |
| Source note | uspto-grants-1978_05 |