Methylcarbamyl fluoride → N-Methyl-N-(n-Octylthiosulfenyl)Carbamoyl Fluoride

HRID 372368Notes

Reaction equation

HRID 372368 reaction equation
[CH2:1]([S:9][S:10]Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:12][NH:13][C:14]([F:16])=[O:15]>C(N(CC)CC)C>[CH3:12][N:13]([S:10][S:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[C:14]([F:16])=[O:15]

Participants

4

Reactant 2

HCID 12545956Methylcarbamyl fluorideHCID 20325288n-Octylthiosulfenylchloride

Product 1

HCID 23333005N-Methyl-N-(n-Octylthiosulfenyl)Carbamoyl Fluoride

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Prepared as above by adding 25.2 g triethylamine to a solution of 48.0 g. n-octylthiosulfenylchloride and 19.26 g N-methylcarbamoyl fluoride. b.p. 110°-118° C/0.2 Torr. ND21 1.4900.

Workup

  1. customPrepared as above

Sources & evidence

ORD record
ord-44a631b71869410598a19aae6c2cc912
Source dataset
uspto-grants-1978_05
Patent number
US04091016

Reaction notes

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